标准摘要
[中文适用范围]: 本文件规定了测定各种来源水中总结合氮(ST-TNb)的方法:地下水、地表水和废水,浓度测量范围通常为 0.5 mg/l 至 220 mg/l使用小规模密封管法制备 ST-TNb。 小型密封管方法可能需要不同的测量范围。 根据不同制造商的小型密封管方法的类型,测量范围可能有所不同。 用户可以选择适合应用范围的小规模密封管,或者通过初步稀释来调整浓度超过测试测量范围的样品。 注:小规模密封管的结果在测试应用范围的中间最为精确。 所有小规模密封管方法均基于加热块中加热的碱性过硫酸钾氧化。 适用不同的消化温度,100°C或120°C或170°C,以及不同的消化时间。 根据所用小型密封管的典型操作程序,应用二甲基苯酚显色反应,参见第 9 条。 [外文原描述]: This document specifies a method for the determination of total bound nitrogen (ST-TN b ) in water of various origins: groundwater, surface water, and wastewater, in a measuring range of concentration generally between 0,5 mg/l and 220 mg/l of ST-TN b using the small-scale sealed tube method. Different measuring ranges of small-scale sealed tube methods can be required. The measuring ranges can vary depending on the type of small-scale sealed tube method of different manufacturers. It is up to the user to choose the small-scale sealed tube with the appropriate application range or to adapt samples with concentrations exceeding the measuring range of a test by preliminary dilution. NOTE The results of a small-scale sealed tube are most precise in the middle of the application range of the test. All small-scale sealed tube methods are based on a heated alkaline potassium persulfate oxidation in a heating block. Different digestion temperatures, 100 °C or 120 °C or 170 °C, and different digestion times are applicable. Dimethylphenol colour reactions are applied, depending on the typical operating procedure of the small-scale sealed tube used, see Clause 9 .
英文名称Water quality — Determination of total bound nitrogen (ST-TNb) in water using small-scale sealed tubes — Part 1: Dimethylphenol colour reaction