标准摘要
[中文适用范围]: 本标准规定了工业用化工产品中以硫酸根表示的痕量硫化合物测定的通用方法——还原和滴定法。 在可采用本方法的化工产品标准中应规定处理试料的方法,以使硫化合物转变为硫酸盐,必要时可 对通用操作步骤进行可能需要的任何改进。 [外文原描述]: Describes a method based on prior conversion of the sulphur compounds in a test portion to sulphate, if required, and reduction of the sulphate ions ti hydrogen sulphide by a mixture of hydriodic and phosphinic acids in the presence of hydrochloric acid. The hydrogen sulphide is entrained in a current of nitrogen and absorbed in a solution of sodium hydroxide in aqueous acetone, followed by titration of the sulphide ions with standard volumetric mercury(II) acetate or nitrate solution in the presence of 1,5-diphenyl-3-thiocarbazone (dithiozone) as indicator.
英文名称Chemical products for industrial use — General method for determination of traces of sulphur compounds, as sulphate, by reduction and titrimetry